Undergraduate Instrumental Analysis
Concepts of Instrumental Analytical ChemistryIntroduction: What is Analytical Chemistry?Analytical ApproachBasic Statistics and Data HandlingSample PreparationPerforming the MeasurementAssessing the DataProblemsBibliographyIntroduction to SpectroscopyInteraction Between Electromagnetic Radiation and MatterAtoms and Atomic SpectroscopyMolecules and Molecular SpectroscopyAbsorption
LawsMethods of CalibrationOptical Systems Used in SpectroscopySpectroscopic Technique and Instrument NomenclatureSuggested experimentsProblemsBibliographyMagnetic Resonance SpectroscopyNuclear Magnetic Resonance Spectroscopy IntroductionThe FTNMR ExperimentChemical ShiftsSpin-Spin CouplingInstrumentationAnalytical Applications of NMRHyphenated NMR TechniquesNMR Imaging and MRITime Domain NMRLow-Field, Portable, and Miniature NMR InstrumentsLimitations of NMRElectron Spin Resonance SpectroscopySuggested ExperimentsProblemsSpectral DatabasesBibliographyInfrared, Near-Infrared, and Raman SpectroscopyAbsorption of IR Radiation by MoleculesIR InstrumentationSampling TechniquesFTIR MicroscopyNondispersive IR SystemsAnalytical Applications of IR SpectroscopyNIR SpectroscopyRaman SpectroscopyChemical Imaging Using NIR, IR, and Raman SpectroscopySuggested ExperimentsProblemsBibliographySpectral DatabasesVisible and Ultraviolet Molecular SpectroscopyIntroductionInstrumentationUV Absorption Spectra of MoleculesUV Spectra and the Structure of Organic MoleculesAnalytical ApplicationsAccuracy and Precision in UV/Vis Absorption SpectrometryNephelometry and TurbidimetryMolecular Emission SpectrometryInstrumentation for Luminescence MeasurementsAnalytical Applications of LuminescenceSuggested ExperimentsProblemsBibliographyAtomic Absorption SpectrometryAbsorption of Radiant Energy by AtomsInstrumentationAtomization ProcessInterferences in AASAnalytical Applications of AASSuggested
ExperimentsProblemsAppendicesBibliographyAtomic Emission SpectroscopyFlame Atomic Emission SpectroscopyAtomic OESPlasma Emission SpectroscopyGD Emission SpectrometryAFSCommercial Atomic Emission SystemsLaser-Induced Breakdown SpectroscopyAtomic Emission Literature and ResourcesComparison of Atomic Spectroscopic and ICP-MS TechniquesSuggested experimentsProblemsAppendicesBibliographyX-Ray Spectroscopy (Contributing authors: Alexander Seyfarth and Eileen Skelly Frame)Origin of X-Ray SpectraX-Ray FluorescenceX-Ray AbsorptionX-Ray DiffractionX-Ray Emission Commercial X-Ray Instrument Manufacturers Suggested ExperimentsProblemsAppendicesBibliographyMass Spectrometry I: Principles and InstrumentationPrinciples of MSInstrumentationIon Mobility SpectrometryProblemsBibliographyMass Spectrometry II: Spectral Interpretation and ApplicationsInterpretation of Mass Spectra: Structural Determination of Simple MoleculesMass Spectral Interpretation: Some ExamplesApplications of Molecular MSAtomic MSProblemsAppendixBibliographyPrinciples of ChromatographyIntroduction to ChromatographyWhat is the Chromatographic Process?Chromatography in More than One DimensionVisualization of the Chromatographic Process at the Molecular Level: Analogy to "People on a Moving Belt Slideway"Digression on the Central Role of Silicon-Oxygen Compounds in ChromatographyBasic Equations Describing Chromatographic SeparationsHow Do Column Variables Affect Efficiency (Plate Height)?Practical Optimization of Chromatographic SeparationsExtra-Column Band Broadening EffectsQualitative Chromatography: Analyte IdentificationQuantitative Measurements in ChromatographyExamples of Chromatographic Calculations ProblemsBibliographyGas ChromatographyHistorical Development of GC: The First Chromatographic InstrumentationAdvances in GC Leading to Present-Day InstrumentationGC Instrument Component Design
(Injectors)GC Instrument Component Design (The Column)GC Instrument Operation (Column Dimensions and Elution Values)GC Instrument Operation (Column Temperature and Elution Values)GC Instrument Component Design (Detectors)Hyphenated GC Techniques (GC-MS, GC-IR, GC-GC, or D-GC)Retention Indices (A Generalization of Relative Rt Information)Scope of GC AnalysesProblemsAppendix 12.1BibliographyChromatography with Liquid Mobile PhasesHigh-Performance Liquid ChromatographyChromatography of Ions Dissolved in LiquidsAffinity ChromatographySize-Exclusion ChromatographySupercritical Fluid ChromatographyElectrophoresisPlanar Chromatography and Planar ElectrophoresisProblems and ExercisesAppendix 13.ABibliographySurface AnalysisIntroductionElectron Spectroscopy TechniquesIon Scattering SpectroscopySecondary Ion Mass SpectrometryElectron Microprobe (Electron Probe Microanalysis)ProblemsBibliographyElectroanalytical ChemistryFundamentals of ElectrochemistryElectrochemical CellsElectroanalytical MethodsLiquid Chromatography DetectorsSpectroelectrochemistryQuartz Crystal MicrobalanceSuggested ExperimentsProblemsAppendix 15.ABibliographyThermal AnalysisThermogravimetryDifferential Thermal AnalysisDifferential Scanning Calorimetry Hyphenated TechniquesThermometric TitrimetryDirect Injection EnthalpimetryMicrocalorimetryThermomechanical Analysis and Dynamic Mechanical AnalysisOptical Thermal AnalysisSummarySuggested ExperimentsProblemsBibliographyAcronyms IndexIndex.
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Podrobná bibliografie
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Hlavní autoři
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Robinson, James W.,
Frame, Eileen Skelly,
Frame II, George M.
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Typ dokumentu
- eBook
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Jazyk
- English
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Vydáno
-
Bosa Roca
CRC Press
2014
Taylor & Francis Group
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Vydání
- 7
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Témata
-
ISBN
- 9781420061352
1420061356
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DOI
- 10.1201/b15921
